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超順磁性四氧化三鐵納米顆粒的制備及表征

Preparation and characterization of super-paramagnetic Fe3O4nanoparticles

作者: 蔡曉峰  張黎明  戴長松 
單位:哈爾濱醫(yī)科大學附屬第一醫(yī)院(哈爾濱150001)
關鍵詞: 超順磁性四氧化三鐵;水熱法;物理化學溶栓 
分類號:
出版年·卷·期(頁碼):2012·31·6(603-606)
摘要:

目的 水熱法制備超順磁性四氧化三鐵納米顆粒,檢測其物理學及磁學性質,并探討其用于物理化學溶栓的可行性。方法 水熱法制備聚乙二醇6000包被的四氧化三鐵顆粒,采用X射線衍射法分析其結構,用掃描電鏡測量其直徑及分布,用振動樣品磁強計檢測磁學參數(shù)。結果 所得樣品為四氧化三鐵晶體,粒徑為200nm,質量飽和磁場強度為79.8emu/g Fe。結論 制備的樣品粒徑均一,分散性好,超順磁性,水溶性好,可用于物理化學溶栓。

Objective To prepare super paramagnetic Fe3O4by hydrothermal method and test the physical and magnetic properties. Methods The Fe3O4 nanoparticles with PEG6000-coating is obtained by means of hydrothermal method,the structure is analyzed by X-ray powder diffraction method,the size and distribution is measured by transmission electron microscope,and the susceptibility is measured by Vibrating Sample Magnetometer dollars. Results The particle diameter size of the super paramagnetic Fe3O4 is 200nm. These particles possess some characteristics of super paramagnetism. The quality saturation magnetic intensity is 79.8emu/g Fe. Conclusions The samples are dispersed,water-soluble,super-paramagnetic and homogeneous in particle diameter,which can be used in physical chemistry thrombolysis.

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